HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexene → HCID 21082866, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexene | HCID 8079 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 2-Chloro-3,5-dinitropyridine | HCID 75738 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21082866 | HCID 21082866 | — |
Reaction Steps
2 g of (1-piperidyl)-3,5-dinitropyridine, obtained according to Protocol A from 2-chloro-3,5-dinitropyridine and piperidine, were reduced by hydrogen transfer in 50 ml of ethanol in the presence of palladium-on-charcoal and 5 ml of cyclohexene. 930 mg of N-(3,5-diaminopyrid-2-yl)piperidine dihydrochloride were thus obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07175670B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-03c5eb8df3444a068ca7ef4870414a09 |
| Source note | uspto-grants-2007_02 |