2-Chloro-3,5-dinitropyridine → HCID 23064287, compound

Participants

Reaction Conditions

Reaction Steps

2 g (9.82 mmol) of 2-chloro-3,5-dinitropyridine, 10 ml of THF and 20 mmol of 3,5-dimethylpiperidine were placed in a round-bottomed flask. he mixture was maintained at 60° C. for 15 hours with stirring and was then poured into a mixture of ice-water with stirring. The precipitate formed was filtered off by suction and dried under vacuum to constant weight. 2.55 g of yellow powder were obtained.

Provenance & Evidence