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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 347637Generated: October 30, 2026

2,3,4,5-tetrahydro-1H-1-benzazepine → HCID 69365105, compound

https://huagongshe.com/reaction/347637

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2,3,4,5-tetrahydro-1H-1-benzazepineHCID 576503—
Reactant4-[[[(1,1-Dimethylethoxy)carbonyl]amino]methyl]-3-nitrobenzoic acidHCID 21083266—
ProductHCID 69365105HCID 69365105—

Reaction Steps

The carboxylic acid from Example B (0.911 g, 3.08 mmol) was reacted with 2,3,4,5-tetrahydro-1H-1-benzazepine (0.453 g, 3.08 mmol) according to the procedure in Example 1A. The product was purified by flash chromatography on silica (eluant EtOAc:pet. ether 50:50); yield 0.58 g (43%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07176195B2
Source datasetuspto-grants-2007_02
ORD IDord-00cf7f27e33546c5b150427a045b2182
Source noteuspto-grants-2007_02