HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Iodoethane → 2H-1,5-Benzodiazepin-2-one, 1,3,4,5-tetrahydro-1-ethyl-
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Iodoethane | HCID 6340 | — |
| Edukt | 2,3,4,5-tetrahydro-1H-1,5-benzodiazepin-2-one | HCID 223771 | — |
| Produkt | 2H-1,5-Benzodiazepin-2-one, 1,3,4,5-tetrahydro-1-ethyl- | HCID 3078200 | — |
Reaktionsschritte
2-Oxo-2,3,4,5-tetrahydro-1H-1,5-benzodiazepine (1.95 g, 11.96 mmol) was reacted with ethyl iodide (1.4 ml, 17.5 mmol) according to the procedure in Example 18A. The product was purified by flash chromatography on silica (eluant EtOAc); yield 1.70 g (75%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07176195B2 |
| Quelldatensatz | uspto-grants-2007_02 |
| ORD ID | ord-c59cc29e10ad497786d80d9cece45616 |
| Quellennotiz | uspto-grants-2007_02 |