HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21083979, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl isocyanate | HCID 8022 | — |
| Reactant | HCID 21083988 | HCID 21083988 | — |
| Product | HCID 21083979 | HCID 21083979 | — |
Reaction Steps
The title compound was prepared from the HCl salt of the compound of Example 81 and ethyl isocyanate following the method described for the compound of Example 97 to give the product as a solid (24 mg). δH (DMSO-d6) 8.59 (1H,s), 7.8–7.4 (11H, m), 6.67 (1H, t, J 5 Hz), 6.38 (1H, d, J 10 Hz), 3.1–2.9 (2H, m), 0.97 (3H, t, J 7 Hz). LCMS (ES+) 390 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07176215B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-f6e81635f45e4dfa9db778aae26e0a93 |
| Source note | uspto-grants-2007_02 |