HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butanol → HCID 69523188, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butanol | HCID 6386 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | [5-(4-Fluorophenylcarbamoyl)pyrimidin-2-yloxy]acetic acid | HCID 21087356 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 69523188 | HCID 69523188 | 8% |
Reaction Steps
The titled compound was prepared from [5-(4-fluorophenylcarbamoyl)pyrimidin-2-yloxy]acetic acid using tert-butyl alcohol (9.6 mg, 0.13 mmol) as the source alcohol. Chromatography (1:1 ethyl acetate:hexane) through SiO2 yielded 5 mg (8%) of the titled compound. ESI-MS m/z 348 (MH+), 346 (M−H−).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07176310B1 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-cec8160f24474e86ba22ffdf07cf233b |
| Source note | uspto-grants-2007_02 |