HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexylamine → HCID 86760391, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | [5-(4-Fluorophenylcarbamoyl)pyrimidin-2-yloxy]acetic acid | HCID 21087356 | — |
| Product | HCID 86760391 | HCID 86760391 | 57% |
Reaction Steps
The titled compound was prepared from [5-(4-fluorophenylcarbamoyl)pyrimidin-2-yloxy]acetic acid using cyclohexylamine (24 μL, 0.21 mmol) as the coupling partner. Concentration (no chromatography) yielded 36 mg (57%) of the titled compound. ESI-MS m/z 373 (MH+), 371 (M−H−).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07176310B1 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-9845525c9305467d8403a0014c286445 |
| Source note | uspto-grants-2007_02 |