HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cinnamoylbenzene → HCID 11481281, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cinnamoylbenzene | HCID 7189 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 11481281 | HCID 11481281 | — |
Reaction Steps
Washed phaseolus aureus L (green grams) 50 g. were taken into a conical flask and allowed to soak in deionised water (400 ml) for a period of 24 hr. Chalcone (0.500 g; 0.0024 moles) (V) was added to the soaked phaseolus aureus L (green grams) in the above water, covered and allowed to shake for 24 hr at 15–20° C. Then the green grams were filtered off and washed with deionised water (3×100 ml). The combined filtrate was extracted with chloroform (3×500 ml). The chloroform layer was dried and the crude product obtained (240 mg). Pure 1,3-diphenyl-(1S)-propan-1-ol (VI) was obtained after column chromatography with silica gel using chloroform as eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07179624B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-62899b36257a4a259e109184053f35e8 |
| Source note | uspto-grants-2007_02 |