HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → N-(3-Amino-4-thienyl)-N'-(2-chloro-6-methylphenyl)thiourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | 2-Chloro-6-Methylphenyl Isothiocyanate | HCID 3731725 | — |
| Reactant | Thiophene-3,4-diamine dihydrobromide | HCID 21989329 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | N-(3-Amino-4-thienyl)-N'-(2-chloro-6-methylphenyl)thiourea | HCID 86037747 | — |
Reaction Steps
was obtained in a similar manner to the method specified in Example 6a) by reacting a mixture prepared from 0.74 g (=1.01 ml) of N-ethyl-N,N-diisopropylamine in 40 ml of THF, 0.8 g of 3,4-diaminothiophene dihydrobromide and 0.473 g of 2-chloro-6-methylphenyl isothiocyanate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07179830B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-b6d010019dc9429985c7dd2cf43e51ec |
| Source note | uspto-grants-2007_02 |