HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → methyl 3-acetamidothiophene-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Methyl 3-amino-2-thiophenecarboxylate | HCID 89652 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | methyl 3-acetamidothiophene-2-carboxylate | HCID 729216 | — |
Reaction Steps
was obtained by reacting 471 g of methyl 3-aminothiophene-2-carboxylate with 226.64 ml of acetic anhydride in 500 ml of toluene. Colorless crystalline product. M.p. 94–95° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07179830B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-20c23600c5dc4855babc10221f36ebf8 |
| Source note | uspto-grants-2007_02 |