Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | methyl 3-acetamidothiophene-2-carboxylate | HCID 729216 | — |
| Product | HCID 22139803 | HCID 22139803 | — |
Reaction Steps
was obtained by reacting 19.9 g of methyl 3-acetylaminothiophene-2-carboxylate in 100 ml of chloroform with 17.9 ml of sulfuryl chloride (SO2Cl2) in 120 ml of chloroform by stirring at 40° C. for 2 hours and subsequently boiling under reflux conditions for 15 minutes. After the solvent had been distilled off, the residue was crystallized in ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07179830B2 |
|---|
| Source dataset | uspto-grants-2007_02 |
|---|
| ORD ID | ord-1be62623a17a47cabd5b61e31375bf48 |
|---|
| Source note | uspto-grants-2007_02 |
|---|
