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HRID34954

反应详情

EQUATION

反应方程式

HRID 34954 的结构方程式

REACTANTS

反应物

2
结构：N#CBr
HCID10476

Cyanogen bromide

CBrN

结构：CN1C[C@@H](NC(=O)OCc2ccccc2)C[C@@H]2c3cccc4[nH]cc(c34)C[C@H]21
HCID70417848

未命名化合物

PRODUCTS

生成物

1
结构：N#CN1C[C@@H](NC(=O)OCc2ccccc2)C[C@@H]2c3cccc4[nH]cc(c34)C[C@H]21
HCID86742331

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClC(Cl)Cl
溶剂HCID6212

Chloroform

CHCl3

PROCEDURE

实验过程

A solution of 29.5 g (79 mM) of 8α-benzyloxycarbonylamino-6-methylergoline obtained from step (a) and 25 g (236 mM) cyanobromide in 600 ml chloroform is stirred for 65 hours at room temperature and finally concentrated on a rotary evaporator to give the heading compound which is dried in a high vacuum.

WORKUP

后处理

  1. concentrationfinally concentrated on a rotary evaporator
  2. customto give the heading compound which
  3. customis dried in a high vacuum