HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 1-Chloro-3-(diethylamino)-2-propanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Reactant | Diethylamine | HCID 8021 | — |
| Product | 1-Chloro-3-(diethylamino)-2-propanol | HCID 5298859 | — |
Reaction Steps
To 2-chloromethyloxirane (95 g, 1.03 mole) was added a mixture of water (3.08 g, 0.17 mole) and diethylamine (106.2 mL, 1.03 mole) at 30° C. The reaction mixture was then stirred at 28–35° C. for 6 hour and cooled to 20–25° C. to give 1-chloro-3-diethylamino-propan-2-ol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07179910B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-2837f6bc744141a89a74fc35b0e9d299 |
| Source note | uspto-grants-2007_02 |