反应详情

In ethanol were dissolved 259 mg (0.72 mmol.) of N-(1-phenyl-3-pyrrolidinopropyl)quinaldinamide and 91 mg of oxalic acid dihydrate. The resulting solution was evaporated under reduced pressure to remove the solvent. The residue was recrystallized from a mixture of acetone (6 ml) and diethyl ether (3 ml) to obtain 310 mg (yield: 96%) of the subject compound as a white crystalline product.

1. customThe resulting solution was evaporated under reduced pressure
2. customto remove the solvent
3. customThe residue was recrystallized from a mixture of acetone (6 ml) and diethyl ether (3 ml)