HRID35002

反应详情

EQUATION

反应方程式

HRID 35002 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

In ethanol were dissolved under heating 1.08 g (3.0 mmol.) of N-(3-diethylamino-1-phenylpropyl)quinaldinamide and 313 mg (3.0 mmol.) of fumaric acid. The resulting solution was evaporated under reduced pressure to remove the solvent. The residue was recrystallized from 8 ml of ethanol to obtain 1.14 g (yield: 88%) of the subject compound as a white crystalline product.

WORKUP

后处理

  1. customThe resulting solution was evaporated under reduced pressure
  2. customto remove the solvent
  3. customThe residue was recrystallized from 8 ml of ethanol