HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fumaric Acid → N-(3-diethylamino-1-phenylpropyl)quinaldinamide fumarate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fumaric Acid | HCID 444972 | — |
| Reactant | N-(3-diethylamino-1-phenylpropyl)quinaldinamide | HCID 67930066 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-(3-diethylamino-1-phenylpropyl)quinaldinamide fumarate | HCID 86742337 | 88% |
Reaction Steps
In ethanol were dissolved under heating 1.08 g (3.0 mmol.) of N-(3-diethylamino-1-phenylpropyl)quinaldinamide and 313 mg (3.0 mmol.) of fumaric acid. The resulting solution was evaporated under reduced pressure to remove the solvent. The residue was recrystallized from 8 ml of ethanol to obtain 1.14 g (yield: 88%) of the subject compound as a white crystalline product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04764617 |
| Source dataset | uspto-grants-1988_08 |
| ORD ID | ord-26141507b2a34f2e83cd0b0a796fa789 |
| Source note | uspto-grants-1988_08 |