Methanol → HCID 131715693, compound

HRID 35015Notes

Reaction equation

HRID 35015 reaction equation
[CH:1](=O)[C:2]1[O:6][CH:5]=[CH:4][CH:3]=1.[CH3:8]O>>[O:6]1[CH:2]=[CH:3][CH:4]=[CH:5]1.[CH3:1][C:2]1[O:6][CH:5]=[CH:4][CH:3]=1.[CH3:8][C:3]1[CH:4]=[CH:5][O:6][C:2]=1[CH3:1]

Participants

3

Reactant 2

HCID 887MethanolHCID 7362Furfural

Product 1

HCID 131715693HCID 131715693, compound

Procedure

Furfural aldehyde and methanol were co-fed in equal amounts over a ZSM-5 zeolite catalyst at atmospheric pressure and at about 500° C. temperature for a residence time of about 1 second. The WHSV ratio was about 25 for each species in the feedstock vapor. The resultant vapor was collected and tested and resulted in a furan/methylfuran/dimethylfuran product ratio of about 5.6/2/1. Therefore, co-feeidng methanol produced substantial methylation of the furan product.

Workup

  1. customfor a residence time of about 1 second
  2. customThe resultant vapor was collected

Sources & evidence

ORD record
ord-1bf441c637544fe88729dd31b7ab1c65
Source dataset
uspto-grants-1988_08
Patent number
US04764627

Reaction notes

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