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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 350642Generated: October 31, 2026

HCID 17817671, compound → HCID 21088905, compound

https://huagongshe.com/reaction/350642

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 17817671HCID 17817671—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductHCID 21088905HCID 2108890583%

Reaction Steps

3-Benzyloxy-6-methoxy-4′-phenoxypicolinanilide was suspended in 5 ml of ethanol. 10% palladium-carbon (30 mg) was added to the suspension. The mixture was subjected to catalytic reduction under atmospheric conditions overnight. The reaction solution was filtered, and the filtrate was concentrated under the reduced pressure. The residue was then purified by column chromatography on silica gel (chloroform) to give the title compound (yield 83%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07183278B1
Source datasetuspto-grants-2007_02
ORD IDord-4e869b2e1ac449d6a87c03c57fc4d859
Source noteuspto-grants-2007_02