HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 17817671, compound → HCID 21088905, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 17817671 | HCID 17817671 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21088905 | HCID 21088905 | 83% |
Reaction Steps
3-Benzyloxy-6-methoxy-4′-phenoxypicolinanilide was suspended in 5 ml of ethanol. 10% palladium-carbon (30 mg) was added to the suspension. The mixture was subjected to catalytic reduction under atmospheric conditions overnight. The reaction solution was filtered, and the filtrate was concentrated under the reduced pressure. The residue was then purified by column chromatography on silica gel (chloroform) to give the title compound (yield 83%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07183278B1 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-4e869b2e1ac449d6a87c03c57fc4d859 |
| Source note | uspto-grants-2007_02 |