HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178418361, compound → HCID 178512074, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Reactant | HCID 178512075 | HCID 178512075 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178512074 | HCID 178512074 | 95.4% |
Reaction Steps
3.47 g (15 mmol) of 1-(4-nitrophenyl)imidazolidin-2-ylidene cyanamide are hydrogenated in 35 ml of methanol using hydrogen on 5% palladium on carbon. Conventional work-up gives 2.88 g of 1-(4-aminophenyl)imidazolidin-2-ylidene cyanamide in the form of a pale-brown solid (ESI: 202).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07183277B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-e5f22fc93b97473980d6ec3ef81dfa9a |
| Source note | uspto-grants-2007_02 |