HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 21957076, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 21027861 | HCID 21027861 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 21957076 | HCID 21957076 | — |
Reaction Steps
[2-(4-Pyridin-2-yl-phenyl)-ethyl]-carbamic acid tert-butyl ester was dissolved in a 1:1 mixture of trifluroacetic acid:dichloromethane. The reaction mixture was stirred at room temperature overnight after which the product was recovered upon solvent removal. The TFA salt was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07183281B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-958ab82382b44ea9b426709fd53303a6 |
| Source note | uspto-grants-2007_02 |