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HRID35072

反应详情

EQUATION

反应方程式

HRID 35072 的结构方程式

REACTANTS

反应物

2
结构：CCOCC
HCID3283

Diethyl Ether

C4H10O

结构：CC(C)(C)CN1C(=O)C2CC(c3ccc([N+](=O)[O-])cc3)(C2)C1=O
HCID20027823

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)CN1C(=O)C2CC(c3ccc(N)cc3)(C2)C1=O
HCID20027838

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Pd]
催化剂HCID23938

Palladium

Pd

结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

In a manner analogous to that described in Example 1a, 4.1 g of 3-neopentyl-1-(4-nitrophenyl)-3-azabicyclo[3.1.1]heptane-2,4-dione are dissolved in 80 ml of ethyl acetate, hydrogenated in the presence of 0.4 g of 5% palladium-on-carbon and worked up. Melting point 141.5°-143° (from diethyl ether).