huagongshe.com
HRID35082

反应详情

EQUATION

反应方程式

HRID 35082 的结构方程式

REACTANTS

反应物

2
结构：CCCN1C(=O)C2(CC(C)C)CC(c3ccc([N+](=O)[O-])cc3)(C2)C1=O
HCID20027837

未命名化合物

结构：CCCCCC.CCOCC
HCID21584099

未命名化合物

PRODUCTS

生成物

1
结构：CCCN1C(=O)C2(CC(C)C)CC(c3ccc(N)cc3)(C2)C1=O
HCID20027841

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Pd]
催化剂HCID23938

Palladium

Pd

结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

In a manner analogous to that described in Example 12a, 5.2 g of 5-isobutyl-1-(4-nitrophenyl)-3-n-propyl-3-azabicyclo[3.1.1]heptane-2,4-dione in 100 ml of ethyl acetate are hydrogenated in the presence of 0.5 g of 5% palladium-on-carbon and worked up. Melting point 86.5°-87° (from n-hexane/ether).