HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-4-fluorobenzenesulphonyl chloride → HCID 178513462, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-4-fluorobenzenesulphonyl chloride | HCID 145222 | — |
| Reactant | 3-Chloro-4-fluorobenzene-1-carboximidamide--hydrogen chloride (1/1) | HCID 2730160 | — |
| Product | HCID 178513462 | HCID 178513462 | — |
Reaction Steps
A mixture of 3-chloro-4-fluorobenzamidine hydrochloride (0.025 g, 0.133 mmol) and 3-chloro-4-fluorophenyl sulfonylchloride (0.0304 g, 0.133 mmol); the title compound is prepared essentially as described in Example 115. ES Positive Ion MS [M+H]+ ions observed: m/z 365 (35Cl, 35Cl), m/z 367 (35Cl, 37Cl) and m/z 369 (37Cl, 37Cl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07183320B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-14e5aae1ba484591954668a36bf67e5e |
| Source note | uspto-grants-2007_02 |