HRID351200
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A mixture of 5-[4-(benzyloxy)phenyl]-1-(4-methoxyphenyl) -N,N-dimethyl-1H-pyrazol-3-amine obtained by Example 15 (0.83 g) and 10% Pd-C 50% wet (160 mg) in acetic acid (8 ml) was hydrogenated under H2 1 atm at room temperature for 10 hrs.
WORKUP
后处理
- customat room temperature
- customfor 10 hrs