HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 21091034, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Trimethylsilyl isocyanate | HCID 70696 | — |
| Reactant | HCID 21090709 | HCID 21090709 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21091034 | HCID 21091034 | — |
Reaction Steps
To a solution of 2-{4-[l-(4-chlorophenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl]phenyl}ethanamine obtained by Example 53 (300 mg) and triethylamine (0.57 ml) in dichloromethane (10 ml) was added dropwise trimethylsilyl isocyanate (0.555 ml) at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07183306B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-379363dc5e1f48b08afa80ebaa8ec9ca |
| Source note | uspto-grants-2007_02 |