HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21090872, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 21090871 | HCID 21090871 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21090872 | HCID 21090872 | — |
Reaction Steps
A mixture of 4-[1-(4-methoxyphenyl)-3-(trifluoro-methyl)-1H-pyrazol-5-yl]benzonitrile obtained by Example 56 (430 mg), Pd/C (100 mg) and 1N hydrochloric acid (1.3 ml) in methanol (43 ml) was stirred under Hydrogen atmosphere for 5 hrs.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07183306B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-a48b3f0be1f148d0a47ab3bd77d046d7 |
| Source note | uspto-grants-2007_02 |