HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66775446, compound → HCID 58807411, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66775446 | HCID 66775446 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Solvent | Heptane | HCID 8900 | — |
| Product | HCID 58807411 | HCID 58807411 | — |
Reaction Steps
0.4 g of 5% Pt/C (dry) is added to a solution of 1.8 g (5.9 mmol) of 2 in 50 ml of heptane, and the mixture is hydrogenated at atmospheric pressure for 20 hours. The solvent is removed under reduced pressure, and the entire amount is converted into 4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07183447B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-c72b2aafb7b64a219d707d1e305b40f9 |
| Source note | uspto-grants-2007_02 |