HCID 66775446, compound → HCID 58807411, compound

HRID 351352Notes

Reaction equation

HRID 351352 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([F:15])[C:5]([CH:9]=[CH:10][C@H:11]([CH3:14])[CH2:12][CH3:13])=[C:6]([F:8])[CH:7]=1>CCCCCCC.[Pt]>[Br:1][C:2]1[CH:7]=[C:6]([F:8])[C:5]([CH2:9][CH2:10][C@H:11]([CH3:14])[CH2:12][CH3:13])=[C:4]([F:15])[CH:3]=1

Participants

4

Reactant 1

HCID 66775446HCID 66775446, compound

Product 1

HCID 58807411HCID 58807411, compound

Reagents, catalysts & solvents 2

HCID 23939PlatinumCatalystHCID 8900HeptaneSolvent

Procedure

0.4 g of 5% Pt/C (dry) is added to a solution of 1.8 g (5.9 mmol) of 2 in 50 ml of heptane, and the mixture is hydrogenated at atmospheric pressure for 20 hours. The solvent is removed under reduced pressure, and the entire amount is converted into 4.

Workup

  1. customThe solvent is removed under reduced pressure

Sources & evidence

ORD record
ord-c72b2aafb7b64a219d707d1e305b40f9
Source dataset
uspto-grants-2007_02
Patent number
US07183447B2

Reaction notes

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