HRID351544

反应详情

EQUATION

反应方程式

HRID 351544 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of 1-benzyloxycarbonyl-4-(4-hexyloxyphenyl)-4-hydroxypiperidine (1.4 g) in methanol (28 ml) was added dry 10% palladium on carbon (0.7 g) and stirred for 6 hours under hydrogen atmosphere. The palladium on carbon was filtered off, and the filtrate was evaporated under reduced pressure to give 4-(4-hexyloxyphenyl)-4-hydroxypiperidine (0.74 g).

WORKUP

后处理

  1. dry with materialdry 10% palladium on carbon (0.7 g)
  2. filtrationThe palladium on carbon was filtered off
  3. customthe filtrate was evaporated under reduced pressure