Ammonium formate → HCID 59892278, compound

Participants

Reaction Steps

The compound of example 46 (104 mg, 0.2 mmol) was hydrogenated by means of ammonium formate (143 mg) and Pd/C (30 mg; 10%) in methanol (10 ml) at room temperature. After 16 h (LC-MS control) the mixture was filtered off and the solvent was removed. Remaining traces of formate were removed in high vacuo at elevated temperature. 47 mg (57%) of the title compound were obtained. MS 370.10 (M+1)+

Provenance & Evidence