Benzoic acid, 4-(acetyloxy)- → p-Acetoxybenzoyl chloride

HRID 351647Notes

Reaction equation

HRID 351647 reaction equation
[C:1]([O:4][C:5]1[CH:13]=[CH:12][C:8]([C:9](O)=[O:10])=[CH:7][CH:6]=1)(=[O:3])[CH3:2].C(Cl)(=O)C([Cl:17])=O>>[C:1]([O:4][C:5]1[CH:13]=[CH:12][C:8]([C:9]([Cl:17])=[O:10])=[CH:7][CH:6]=1)(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 16865Benzoic acid, 4-(acetyloxy)-HCID 65578Oxalyl chloride

Product 1

HCID 2756254p-Acetoxybenzoyl chloride

Procedure

A mixture of 4-acetoxybenzoic acid (516 mg) and oxalyl chloride (0.5 ml) was stirred for 30 minutes. The mixture was concentrated under reduced pressure to give 4-acetoxybenzoyl chloride.

Workup

  1. concentrationThe mixture was concentrated under reduced pressure

Sources & evidence

ORD record
ord-f5d5a85b399d431889f7664f51e6b192
Source dataset
uspto-grants-2004_06
Patent number
US06743793B2

Reaction notes

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