反应详情

温度

85 °C

6.65 g (40 mmol) of ethyl methanesulphonylacetate and 5.72 g (48 mmol) of N,N-dimethylformamide dimethyl acetal are admixed and heated at 85° C. overnight. The solution is concentrated using a rotary evaporator, and the solid is comminuted with cyclohexane and filtered off with suction.

1. concentrationThe solution is concentrated
2. customa rotary evaporator
3. customthe solid is comminuted with cyclohexane
4. filtrationfiltered off with suction