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n-Isopropyl-1-[3-(trimethylsilylethynyl)phenyl]-1,4-dihydro[1,8]naphthyridin-4-one-3-carboxamide → 2-(6-Ethynylpyridin-3-yl)propan-2-ol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | n-Isopropyl-1-[3-(trimethylsilylethynyl)phenyl]-1,4-dihydro[1,8]naphthyridin-4-one-3-carboxamide | HCID 22714290 | — |
| 反応物 | 5-(1-Hydroxy-1-methylethyl)-2-[(trimethylsilyl)ethynyl]pyridine | HCID 22714299 | — |
| 生成物 | 2-(6-Ethynylpyridin-3-yl)propan-2-ol | HCID 22714296 | — |
反応手順
Following the procedure of Step 2 of EXAMPLE 5, but substituting the product 5-(1-hydroxy-1-methylethyl)-2-[(trimethylsilyl)ethynyl]pyridine from present Step 2 for N-isopropyl-1-[3-(trimethylsilylethynyl)phenyl]-1,4-dihydro[1,8]naphthyridin-4-one-3-carboxamide, the 2-ethynyl-5-(1-hydroxy-1-methylethyl)pyridine compound was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06743802B2 |
| 出典データセット | uspto-grants-2004_06 |
| ORD ID | ord-40c2f292567c4d3483f2f4e1a8f78178 |
| 出典メモ | uspto-grants-2004_06 |