HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetylene → HCID 22714305, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetylene | HCID 10821 | — |
| Reactant | Trimethylsilylacetylene | HCID 66111 | — |
| Reactant | 1-(3-bromophenyl)-N-isopropyl-4-oxo-1,4-dihydro-1,8-naphthyridine-3-carboxamide | HCID 12991318 | — |
| Product | HCID 22714305 | HCID 22714305 | — |
Reaction Steps
Following the procedure of Step 5 of EXAMPLE 1, but substituting the 1-(3-Bromophenyl)-1,4-dihydro[1,8]naphthyridin-4-one-3-carboxamide from present Step 1 for N-isopropyl-1-(3-bromophenyl)-1,4-dihydro[1,8]naphthyridin-4-one-3-carboxamide and trimethylsilylacetylene for phenylacetylene, the 1-[3-(trimethylsilylethynyl)phenyl]-1,4-dihydro[1,8]naphthyridin-4-one-3-carboxamide product was obtained as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06743802B2 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-a9eed907b4114b7fa532b6ca4ea1b9ee |
| Source note | uspto-grants-2004_06 |