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HRID35178

反应详情

EQUATION

反应方程式

HRID 35178 的结构方程式

REACTANTS

反应物

3
结构：[Na+].[OH-]
HCID14798

Sodium Hydroxide

HNaO

结构：O=C1COc2ccccc2N1
HCID72757

2H-1,4-Benzoxazin-3(4H)-one (8CI)(9CI)

C8H7NO2

结构：B#B
HCID6328200

Boron, mol. (B2)

B2

PRODUCTS

生成物

1
结构：c1ccc2c(c1)NCCO2
HCID585096

Benzomorpholine

C8H9NO

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

3,4-Dihydro-3-oxo-1,4(2H)-benzoxazine was refluxed for several hours in one equivalent of diborane in tetrahydrofuran. Excess sodium hydroxide solution was added, the product was extracted with ether and the solvent was evaporated to give the title compound as an oil.

WORKUP

后处理

  1. extractionthe product was extracted with ether
  2. customthe solvent was evaporated