HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Methylsulfonyl)aniline → HCID 10881660, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Methylsulfonyl)aniline | HCID 79617 | — |
| Reactant | 4-Isopropoxybenzaldehyde | HCID 250077 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 10881660 | HCID 10881660 | — |
Reaction Steps
A mixture of 1.04 g (6.09 mmol) of 4-methylsulfonylaniline (obtained in reference example 1), 1.00 mL (6.09 mmol) of 4-isopropoxybenzaldehyde (obtained in reference example 3) and 25 mL of toluene was heated at reflux in a Dean-Stark for 2 days. The solvent was removed and the crude product obtained was directly used in the next reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06743816B2 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-20e480c20fc7491b9b4b97c165a31d95 |
| Source note | uspto-grants-2004_06 |