HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22714705, compound → HCID 22714704, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22714705 | HCID 22714705 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 22714704 | HCID 22714704 | — |
Reaction Steps
9.74 g of methyl 5-nitro-1-benzocyclobutanecarboxylate are hydrogenated for 6 hours 30 minutes, at ambient temperature and atmospheric pressure, in the presence of 10% Pd/C. After filtration and concentration under reduced pressure, the expected product is isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06743818B2 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-356fc177bc7846cdac2ccd035550752c |
| Source note | uspto-grants-2004_06 |