HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-3-nitropyridine → HCID 22714503, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-3-nitropyridine | HCID 79613 | — |
| Reactant | HCID 22714435 | HCID 22714435 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 22714503 | HCID 22714503 | — |
Reaction Steps
Analogously to Example 18, the compound 35, prepared in accordance with Example 14.2, is reacted with 2-chloro-3-nitropyridine and triethylamine, giving 3-{6-[3-(3-nitropyridin-2-ylamino)propoxy]-1H-indol-3-yl}-3-phenylpropionic acid. After preparative HPLC: 3-{6-[3-(3-nitropyridin-2-yl-amino)propoxy]-1H-indol-3-yl}-3-phenylpropionic acid trifluoroacetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06743810B2 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-504f0b48df1341609e4bf06d314c3936 |
| Source note | uspto-grants-2004_06 |