HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → HCID 86587405, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | HCID 11486828 | HCID 11486828 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 86587405 | HCID 86587405 | — |
Reaction Steps
2 g (4.8 mmol) of the internal salt 46 are dissolved in 5 ml of dioxane and stirred for 2 hours at RT with 310 μl (4.8 mmol) of methanesulfonic acid in 5 ml of water. The solution is subsequently evaporated, giving (3S)-3-phenyl-3-{6-[3-(pyridin-2-ylamino)propoxy]indol-3-yl}propionic acid methanesulfonate after freeze-drying from acetonitrile/water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06743810B2 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-6a9001ec1d0148c58ffe7199be494a92 |
| Source note | uspto-grants-2004_06 |