HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → Benzoxazines
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | (3-Aminopropyl)triethoxysilane | HCID 13521 | — |
| Reactant | 4-Dodecylphenol | HCID 66030 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Benzoxazines | HCID 17845026 | — |
Reaction Steps
This benzoxazine was prepared from 4-dodecylphenol (26.2 g, 100 mmol), 3-aminopropyltriethoxysilane (22.1 g, 100 mmol), paraformaldehyde (6.3 g, 210 mmol), and toluene (150 mL). The method to prepare this compound was the same as that used to make the previous benzoxazines. The final product was a clear, faint yellow liquid. The yield was 92%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06743852B2 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-5c4fb0813f0f43eca98b767701a6525b |
| Source note | uspto-grants-2004_06 |