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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 351958Generated: October 25, 2026

Formaldehyde → Benzoxazines

https://huagongshe.com/reaction/351958

Reaction equation

Participants

RoleNameHCIDCharge
ReactantFormaldehydeHCID 712—
Reactant(3-Aminopropyl)triethoxysilaneHCID 13521—
Reactant4-DodecylphenolHCID 66030—
SolventTolueneHCID 1140—
ProductBenzoxazinesHCID 17845026—

Reaction Steps

This benzoxazine was prepared from 4-dodecylphenol (26.2 g, 100 mmol), 3-aminopropyltriethoxysilane (22.1 g, 100 mmol), paraformaldehyde (6.3 g, 210 mmol), and toluene (150 mL). The method to prepare this compound was the same as that used to make the previous benzoxazines. The final product was a clear, faint yellow liquid. The yield was 92%.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06743852B2
Source datasetuspto-grants-2004_06
ORD IDord-5c4fb0813f0f43eca98b767701a6525b
Source noteuspto-grants-2004_06