Formaldehyde → Benzoxazines

HRID 351958Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 351958
[CH2:1]([C:13]1C=C[C:16]([OH:19])=[CH:15][CH:14]=1)CCCCCCCCCCC.[NH2:20][CH2:21][CH2:22][CH2:23][Si](OCC)(OCC)OCC.C=O>C1(C)C=CC=CC=1>[O:19]1[C:16]2[CH:15]=[CH:14][CH:13]=[CH:1][C:23]=2[CH:22]=[CH:21][NH:20]1

Komponenten

5

Edukt 3

HCID 712FormaldehydeHCID 13521(3-Aminopropyl)triethoxysilaneHCID 660304-Dodecylphenol

Produkt 1

HCID 17845026Benzoxazines

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 1140TolueneLösungsmittel

Versuchsvorschrift

This benzoxazine was prepared from 4-dodecylphenol (26.2 g, 100 mmol), 3-aminopropyltriethoxysilane (22.1 g, 100 mmol), paraformaldehyde (6.3 g, 210 mmol), and toluene (150 mL). The method to prepare this compound was the same as that used to make the previous benzoxazines. The final product was a clear, faint yellow liquid. The yield was 92%.

Aufarbeitung

  1. customThe method to prepare this compound

Quellen und Nachweise

ORD-Eintrag
ord-5c4fb0813f0f43eca98b767701a6525b
Quelldatensatz
uspto-grants-2004_06
Patentnummer
US06743852B2

Notizen zur Reaktion

Wird geladen…