HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 15612245, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-(3-Pyridylmethyl)naphthalene-6-carboxylic acid hydrochloride | HCID 70407832 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 15612245 | HCID 15612245 | — |
Reaction Steps
A suspension of 2-(3-pyridylmethyl)naphthalene-6-carboxylic acid hydrochloride in 100 ml of methylene chloride is stirred with a stoichiometric amount of dilute aqueous sodium hydroxide solution until the salt is completely dissolved. The organic layer is separated, washed with water, dried over magnesium sulfate and evaporated to yield 2-(3-pyridylmethyl)naphthalene-6-carboxylic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04766127 |
| Source dataset | uspto-grants-1988_08 |
| ORD ID | ord-3af67bb12ea247339371119e2a5e933d |
| Source note | uspto-grants-1988_08 |