Hydrochloric Acid → HCID 86741552, compound

HRID 35200Notes

Reaction equation

HRID 35200 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[C:7]([O:9][S:10]([CH3:13])(=[O:12])=[O:11])[CH:6]=[CH:5][C:4]=1[C:14]1[NH:15][C:16]2[CH:21]=[CH:20][N:19]=[C:18]([O:22]S(C)(=O)=O)[C:17]=2[N:27]=1.[ClH:28]>>[ClH:28].[CH3:1][O:2][C:3]1[CH:8]=[C:7]([O:9][S:10]([CH3:13])(=[O:12])=[O:11])[CH:6]=[CH:5][C:4]=1[C:14]1[N:27]=[C:17]2[C:18](=[O:22])[NH:19][CH2:20][CH:21]=[C:16]2[N:15]=1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 13392820HCID 13392820, compound

Product 1

HCID 86741552HCID 86741552, compound

Procedure

0.65 g of 2-(2-methoxy-4-methanesulfonyloxy-phenyl)-4-methanesulfonyloxy-imidazo [4,5-c]pyridine was dissolved in 35 ml of ethanolic hydrochloric acid, and the solution was stirred for an hour at room temperature. The precipitate which had formed was suction-filtered off and washed with ethanol. Yield: 0.53 g (91% of theory). Melting point: 193°-195° C. (decomp.).

Workup

  1. customThe precipitate which had formed
  2. filtrationwas suction-filtered off
  3. washwashed with ethanol

Sources & evidence

ORD record
ord-817e0e53cce84a688addfa1c94f3d561
Source dataset
uspto-grants-1988_08
Patent number
US04766130

Reaction notes

Loading…