HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(2,3alpha-Dihydro-13-nitro-6-n-propyl-8alpha-ergolinyl)-1,1-diethylurea → 3-(2,3alpha-Dihydro-6-methyl-13-nitro-8beta-ergolinyl)-1,1-diethylurea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(2,3alpha-Dihydro-13-nitro-6-n-propyl-8alpha-ergolinyl)-1,1-diethylurea | HCID 86742346 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 3-(2,3alpha-Dihydro-6-methyl-13-nitro-8beta-ergolinyl)-1,1-diethylurea | HCID 86742345 | 50% |
Reaction Steps
3-(2,3α-Dihydro-13-nitro-6-n-propyl-8α-ergolinyl)-1,1-diethylurea. Yield: 50%. [α]D =-156° (0.5% in CHCl3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04766128 |
| Source dataset | uspto-grants-1988_08 |
| ORD ID | ord-9b40b7ba300a496684bbb24b03014956 |
| Source note | uspto-grants-1988_08 |