HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Furaldehyde → 1-(3-Furanyl)-1,4-butanediol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Furaldehyde | HCID 10351 | — |
| Reactant | 1-(3-Thienyl)-1,4-butanediol | HCID 22715090 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 1-(3-Furanyl)-1,4-butanediol | HCID 13521242 | — |
Reaction Steps
The Grignard reagent prepared in Example 26 step (a) (0.7M, 28 ml, 19.6 mmol) and furan-3-carboxaldehyde (1.92 g, 20 mmol) in anhydrous tetrahydrofuran (15 ml) were used to prepare the title compound, using the procedure described in Example 26 step (a). The product was a colourless oil (2.42 g, 79%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06743939B2 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-67b58915a98543c68995a3e7b8e48989 |
| Source note | uspto-grants-2004_06 |