HuagongsheHuagongshe Chemistry Print Report · For research reference only
Furfural → 1-(2-Furyl)-1,4-butanediol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Furfural | HCID 7362 | — |
| Reactant | 1-(3-Thienyl)-1,4-butanediol | HCID 22715090 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 1-(2-Furyl)-1,4-butanediol | HCID 13815534 | — |
Reaction Steps
The Grignard reagent prepared in Example 26 step (a) (0.7 M, 28 ml, 19.6 mmol), and furan-2-carboxaldehyde (1.92 g, 20 mmol) in anhydrous tetrahydrofuran (15 ml) were used to prepare the sub-title compound, using the procedure described in Example 26 step (a). The product was a colourless oil (2.69 g, 88%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06743939B2 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-51b020c78196475d8b72e615693d5058 |
| Source note | uspto-grants-2004_06 |