N-Phenyl-p-phenylenediamine → 195133-09-6

HRID 352328Notes

Reaction equation

HRID 352328 reaction equation
[C:1]1([NH:7][C:8]2[CH:13]=[CH:12][C:11]([NH2:14])=[CH:10][CH:9]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:15]1(=[O:21])[O:20][C:18](=[O:19])[CH2:17][CH2:16]1>>[NH:7]([C:8]1[CH:13]=[CH:12][C:11]([NH:14][C:15](=[O:21])[CH2:16][CH2:17][C:18]([OH:20])=[O:19])=[CH:10][CH:9]=1)[C:1]1[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

3

Reactant 2

HCID 7564N-Phenyl-p-phenylenediamineHCID 7922Succinic anhydride

Product 1

HCID 3582838195133-09-6

Procedure

The experimental protocol used is the same as that described in J. Amer. Chem. Soc. (1951) 73, 4007, starting from N1-phenyl-1,4-benzenediamine and succinic anhydride in order to produce a pale grey-blue powder. Melting point: 175-176° C.

Workup

  1. customto produce a pale grey-blue powder

Sources & evidence

ORD record
ord-ff6e725ba9404601858d5401af3031ab
Source dataset
uspto-grants-2004_06
Patent number
US06747024B1

Reaction notes

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