HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 19900649, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 22711584 | HCID 22711584 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19900649 | HCID 19900649 | — |
Reaction Steps
3.6 ml (46 mmol) of trifluoroacetic acid is added to a solution of 1.56 g (4.64 mmol) of tert-butyl 2-[3,5-di(tert-butyl)-4-hydroxyphenoxy]acetate (prepared according to J. Heterocycl. Chem. (1994) 31, 1439-1443) in 20 ml of dichloromethane. The reaction mixture is stirred for 1 hour, concentrated under vacuum and the residue is dissolved in
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06747024B1 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-b9d38a97da48402ca6da0467bdb1c0b3 |
| Source note | uspto-grants-2004_06 |