HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 69836129, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | cis-1-Acetyl-5-methoxy-6-(3,4,5-trimethylpiperazin-1-yl)indoline | HCID 69663924 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 69836129 | HCID 69836129 | 101.7% |
Reaction Steps
A stirred solution of D2 (1.6 g, 5 mmole) in 2M HCl acid (50 ml) was heated under reflux for 2 h, then the solution was allowed to cool, basified with K2CO3 and extracted with DCM. The extract was dried (Na2SO4) and concentrated under vacuum to afford the title compound as a pale orange solid (1.4 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06747030B1 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-41808262877a4ec3ab2ce1bda0b03c5a |
| Source note | uspto-grants-2004_06 |