HRID35246

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID2723790

Thiourea

CH4N2S

HCID13626973

2-Bromo-1-(3-bromo-1,2-oxazol-5-yl)ethan-1-one

C5H3Br2NO2

PRODUCTS

生成物

HCID14814698

4-(3-Bromo-5-isoxazolyl)-2-thiazolamine

C6H4BrN3OS

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

A mixture of 32.4 g (120.4 mol) of 5-bromoacetyl-3-bromoisoxazole and 18.4 g (240 mmol) of thiourea in 400 ml of anhydrous ethanol was refluxed for 90 minutes.

WORKUP

后处理

temperaturewas refluxed for 90 minutes